Periodic Table

Proficiency Testing:

As part of our commitment to producing quality results, Lambton Scientific participates in the CALA (Canadian Association for Laboratory Accreditation) administered Proficiency Testing (PT) program. This prgram is considered one of the fundamental cornerstones of our Quality Management Program and a vital mechanism for continuous improvement efforts. Lambton Scientific participates in all existing PT programs for the tests/analytes that we commonly perform and ultimately report to our clients. Samples with unknown concentrations of specific target parameters (inorganics, metals, organics) are analyzed by members within this association using established in-house analytical procedures. As a testament to our growth in size and scope of capabilities, Lambton Scientific has increased from 15 parameters of proficiency testing in 1999 to 63 in 2003 to 96 in 2007 to 118 presently (see table below for our latest results). Also, we are also committed to adding any new parameters that CALA makes available, if that analyte is something we routinely report.

Sets of PT samples are sent out to participating laboratories and each set consists of four individual samples with a diverse range of concentrations.  Samples are received quarterly (spring/fall for conventionals and aqueous metals; summer/Summer for organics and soil metals).  In many cases, the PT samples to be analyzed are complex, real world and/or fortified matrices (i.e. municipal wastewaters, soils/sediments, etc) as opposed to simply fortified, distilled water samples.  The complex nature of these PT samples can provide laboratories with valuable information as to the effects of sample matrix on the reported analytical results.  Results are mathematically compared to consensus values to produce a Proficiency  Test Score.  Based on the scoring for the individual tests or analytes, laboratories are considered to have one of three possible outcomes or status:  "Proficient" (PT Score > 70%), or under "Possible Suspension" (one time PT Score of < 70%) or "Suspended" (two consecutive PT scores of < 70%).  Another strength for this program is the important ramifications associated with a PT score of < 70%.  In these cases corrective actions are required in a timely manner.  A Corrective Action Report (CAR) is automatically triggered, as a mechanism to study any deficiencies in the analytical method / procedure,  rectify the deficiency, and ultimately lead to continuous improvement. A monetary fine is also imposed for parameter suspensions.  For more information on the CALA PT program, please visit their website at http://www.cala.ca/pt_program.html.

CALA PROFICIENCY TESTING (PT) SCORES (Updated Aug 25th, 2010)



Type Parameter
Test Group
Method
Percentage
Last
Conventional Inorganics Alkalinity (pH 4.5)
C-1A
Titrimetric
92
Spring 2010
Ammonia
C-1B
Ion Selective Electrode
84
Spring 2010
BOD5
C-4B
D.O. Meter
85
Spring 2010
Chloride
C-1A
Ion Chromatography
93
Spring 2010
Conductivity (25°C)
C-1A
Conductivity Meter
89
Spring 2010
Cyanide (SAD)
C14
Distillation SIE
94
Spring 2010
DOC  (Dissolved Organic Carbon)
C-1B
IR - Combustion
95
Spring 2010
Fluoride
C-1A
Ion Selective Electrode
80
Fall 2009
Fluoride
C-1A
Ion Chromatography
92
Fall 2009
Nitrate
C-1A
Ion Chromatography
93
Spring 2010
Nitrite + Nitrate
C-1A
Ion Chromatography
92
Spring 2010
pH
C4A
pH Meter
95
Spring 2010
Sulfate
C-1A
Ion Chromatography
93
Spring 2010
TKN (Total Kjeldahl Nitrogen)
C-3
Auto Colour - Digestion
93
Spring 2010
TP (Total Phosphorus)
C-3
Auto Colour - Digestion
81
Spring 2010
TP (Total Phosphorus)
C-3
ICP
82
Spring 2010
TSS (Total Suspended Solids)
C-4A
Gravimetric
79
Spring 2010
TDS (Total Dissolved Solids)
C-15
Gravimetric
97
Spring 2010
Total Phenolics
C33
Colourmetric
93
Spring 2010
O&G (Total Oil and Grease)
C34
Gravimetric
91
Summer 2010
Metals Al - Aluminum (High)
C02B
ICP
97
Spring 2010
Ba - Barium (High)
C02B
ICP
94
Spring 2010
B - Boron (High)
C02B
ICP
96
Spring 2010
Ca - Calcium
C-1A
ICP
82
Spring 2010
Cr - Chromium (High)
C02B
ICP
97
Spring 2010
Co - Cobalt (High)
C02B
ICP
97
Spring 2010
Cu - Copper (High)
C02B
ICP
96
Spring 2010
Fe - Iron (High)
C02B
ICP
96
Spring 2010
Pb - Lead (High)
C02B
ICP
98
Spring 2010
Mg - Magnesium
C-1A
ICP
88
Spring 2010
Mn - Manganese (High)
C02B
ICP
93
Spring 2010
Hg - Mercury
C-19
Cold Vapour AA - Digestion
96
Spring 2010
Mo - Molybdenum (High)
C02B
ICP
94
Spring 2010
Ni - Nickel (High)
C02B
ICP
99
Spring 2010
K - Potassium
C-1A
ICP
92
Spring 2010
Na - Sodium
C-1A
ICP
92
Spring 2010
Sr - Strontium (High)
C02B
ICP
92
Spring 2010
Tl - Thallium (High)
C02B
ICP
96
Spring 2010
Ti - Titanium (High)
C02B
ICP
97
Spring 2010
V - Vanadium (High)
C02B
ICP
96
Spring 2010
Zn - Zinc (High)
C02B
ICP
98
Spring 2010
Al - Aluminum (Soil)
C-17
ICP - Digestion
94
Summer 2010
Sb - Antimony (Soil)
C-17
ICP - Hydride
93
Summer 2010
Ar - Arsenic (Soil)
C-17
ICP - Hydride
96
Summer 2010
Cd - Cadmium (Soil)
C-17
ICP - Digestion
93
Summer 2010
Cr - Chromium (Soil)
C-17
ICP - Digestion
92
Summer 2010
Co - Cobalt (Soil)
C-17
ICP - Digestion
94
Summer 2010
Cu - Copper (Soil)
C-17
ICP - Digestion
89
Summer 2010
Fe - Iron (Soil)
C-17
ICP - Digestion
94
Summer 2010
Pb - Lead (Soil)
C-17
ICP - Digestion
94
Summer 2010
Hg - Mercury (Soil)
C-17
Cold Vapour AA - Digestion
92
Summer 2010
Ni - Nickel (Soil)
C-17
ICP - Digestion
92
Summer 2010
Zn - Zinc (Soil)
C-17
ICP - Digestion
86
Summer 2010
Organics Benzene - (VOC)
C-16
GC/MS - Purge & Trap
95
Summer 2010
Bromodichloromethane - (VOC)
C-16
GC/MS - Purge & Trap
93
Summer 2010
Bromoform - (VOC)
C-16
GC/MS - Purge & Trap
98
Summer 2010
Carbon Tetrachloride - (VOC)
C-16
GC/MS - Purge & Trap
96
Summer 2010
Chlorobenzene - (VOC)
C-16
GC/MS - Purge & Trap
96
Summer 2010
Chlorodibromomethane - (VOC)
C-16
GC/MS - Purge & Trap
94
Summer 2010
Chloroform - (VOC)
C-16
GC/MS - Purge & Trap
95
Summer 2010
1,1-Dichloroethylene - (VOC)
C-16
GC/MS - Purge & Trap
98
Summer 2010
1,2-Dichlorobenzene - (VOC)
C-16
GC/MS - Purge & Trap
90
Summer 2010
1,2-Dichloroethane - (VOC)
C16
GC/MS - Purge & Trap
97
Summer 2010
1,4-Dichlorobenzene - (VOC)
C-16
GC/MS - Purge & Trap
94
Summer 2010
Dichloromethane - (VOC)
C-16
GC/MS - Purge & Trap
88
Summer 2010
Ethylbenzene - (VOC)
C-16
GC/MS - Purge & Trap
97
Summer 2010
Methyl Ethyl Ketone (MEK) - (VOC)
C-16
GC/MS - Purge & Trap
92
Summer 2010
Styrene - (VOC)
C-16
GC/MS - Purge & Trap
95
Summer 2010
Tetrachloroethylene - (VOC)
C-16
GC/MS - Purge & Trap
94
Summer 2010
Toluene - (VOC)
C-16
GC/MS - Purge & Trap
97
Summer 2010
Trichloroethylene - (VOC)
C-16
GC/MS - Purge & Trap
94
Summer 2010
m&p-Xylene - (VOC)
C-16
GC/MS - Purge & Trap
94
Summer 2010
o-Xylene - (VOC)
C-16
GC/MS - Purge & Trap
96
Summer 2010
Vinyl Chloride - (VOC)
C-16
GC/MS - Purge & Trap
96
Summer 2010
Acenaphthene - (S-VOC)
C-07
GC/MS - Extraction
73
Summer 2010
Acenaphthylene - (S-VOC)
C-07
GC/MS - Extraction
74
Summer 2010
Anthracene - (S-VOC)
C-07
GC/MS - Extraction
91
Summer 2010
Benzo (a) anthracene  - (S-VOC)
C-07
GC/MS - Extraction
89
Summer 2010
Benzo (a) pyrene - (S-VOC)
C-07
GC/MS - Extraction
93
Summer 2010
Benzo (b) fluoranthene - (S-VOC)
C-07
GC/MS - Extraction
92
Summer 2010
Benzo (g,h,i) perylene - (S-VOC)
C-07
GC/MS - Extraction
92
Summer 2010
Benzo (k) fluoranthene - (S-VOC)
C-07
GC/MS - Extraction
92
Summer 2010
Chrysene - (S-VOC)
C-07
GC/MS - Extraction
92
Summer 2010
Dibenzo (a,h) anthracene - (S-VOC)
C-07
GC/MS - Extraction
91
Summer 2010
Fluoranthene - (S-VOC)
C-07
GC/MS - Extraction
86
Summer 2010
Fluorene - (S-VOC)
C-07
GC/MS - Extraction
75
Summer 2010
Indeno (1,2,3-cd) pyrene - (S-VOC)
C-07
GC/MS - Extraction
92
Summer 2010
Naphthalene - (S-VOC)
C-07
GC/MS - Extraction
75
Summer 2010
Phenanthrene - (S-VOC)
C-07
GC/MS - Extraction
80
Summer 2010
Pyrene - (S-VOC)
C-07
GC/MS - Extraction
84
Summer 2010
Benzene (Soil)
C-31A
GC/MS - Purge & Trap
89
Summer 2010
Toluene (Soil)
C-31A
GC/MS - Purge & Trap
93
Summer 2010
Ethylbenzene (Soil)
C-31A
GC/MS - Purge & Trap
93
Summer 2010
m/p-Xylene (Soil)
C-31A
GC/MS - Purge & Trap
93
Summer 2010
o-Xylene (Soil)
C-31A
GC/MS - Purge & Trap
96
Summer 2010
PHC - F1: C6-C10 (Soil)
C-31A
GC/FID
99
Summer 2010
PHC - F2: C10-C16 (Soil)
C-31B
GC/FID
88
Summer 2010
PHC - F3: C16-C34 (Soil)
C-31B
GC/FID
83
Summer 2010
PHC - F4: C34-C50 (Soil)
C-31B
GC/FID
76
Summer 2010
Benzene (Soil)
C-36
GC/MS - Purge & Trap
94
Summer 2010
Bromodichloromethane (Soil)
C-36
GC/MS - Purge & Trap
93
Summer 2010
Bromoform (Soil)
C-36
GC/MS - Purge & Trap
93
Summer 2010
Carbon Tetrachloride (Soil)
C-36
GC/MS - Purge & Trap
92
Summer 2010
Chlorobenzene (Soil)
C-36
GC/MS - Purge & Trap
86
Summer 2010
Chlorodibromomethane (Soil)
C-36
GC/MS - Purge & Trap
98
Summer 2010
Chloroform (Soil)
C-36
GC/MS - Purge & Trap
92
Summer 2010
1,1-Dichloroethylene (Soil)
C-36
GC/MS - Purge & Trap
91
Summer 2010
1,2-Dichlorobenzene (Soil)
C-36
GC/MS - Purge & Trap
96
Summer 2010
1,2-Dichloroethane (Soil)
C-36
GC/MS - Purge & Trap
91
Summer 2010
1,4-Dichlorobenzene (Soil)
C-36
GC/MS - Purge & Trap
94
Summer 2010
Dichloromethane (Soil)
C-36
GC/MS - Purge & Trap
92
Summer 2010
Ethylbenzene (Soil)
C-36
GC/MS - Purge & Trap
89
Summer 2010
Methyl Ethyl Ketone (MEK) (Soil)
C-36
GC/MS - Purge & Trap
96
Summer 2010
Styrene (Soil)
C-36
GC/MS - Purge & Trap
96
Summer 2010
Tetrachloroethylene (Soil)
C-36
GC/MS - Purge & Trap
94
Summer 2010
Toluene (Soil)
C-36
GC/MS - Purge & Trap
94
Summer 2010
Trichloroethylene (Soil)
C-36
GC/MS - Purge & Trap
90
Summer 2010
m&p-Xylene (Soil)
C-36
GC/MS - Purge & Trap
93
Summer 2010
o-Xylene (Soil)
C-36
GC/MS - Purge & Trap
93
Summer 2010

NOTES:
CALA Proficiency Testing (PT) recognition if PT score for the specified parameter is 70% or more.


Click here for a direct link to www.cala.ca statistics for Lambton Scientific.